Gerald Gübitz, Martin G. Schmid's Chiral Separations: Methods and Protocols PDF

By Gerald Gübitz, Martin G. Schmid

ISBN-10: 1588291502

ISBN-13: 9781588291509

Tools for enantiomer separation are vitally important for controlling synthesis, for checking race-mization, for enantiomeric purity keep watch over, and for pharmacokinetic reviews. In Chiral Separations: equipment and Protocols, in demand specialists from world wide element the chromatographic and electroseparation thoughts they've got constructed for chiral separations on an analytical scale. defined in step by step element to make sure profitable experimental effects, the methods are awarded as both basic tools or as particular functions to substance periods and designated compounds, with emphasis on excessive functionality liquid chromatography and capillary electrophoresis suggestions, but additionally together with skinny layer chromotographic, fuel chromatographic, and supercritical fluid chromatographic in addition to contemporary electrochromotographic options. each one totally established protocol comprises an creation to the primary underlying the strategy, gear and reagent lists, and precious notes on troubleshooting and heading off recognized pitfalls. updated and hugely useful, Chiral Separations: equipment and Protocols may help either beginner and complex clients not just select optimum tools for his or her separation difficulties, but additionally with ease receive winning effects.

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Extra resources for Chiral Separations: Methods and Protocols

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Chiral separations with aqueous solvents and liquid-liquid systems. J. Chromatogr. 635, 346–348. 84. Xuan, H. T. K. and Lederer, M. (1993) Adsorption chromatography on cellulose. X. Adsorption of tryptophan and derivatives from CuSO4-containing eluents. J. Chromatogr. 645, 185–188. 85. Xuan, H. T. K. and Lederer, M. (1994) Adsorption chromatography on cellulose. XI. Chiral separations with aqueous solutions of cyclodextrins as eluents. J. Chromatogr. 659, 191–197. 86. Suedee, R. and Heard, C. M.

Paris, R. , and Semonsky, M. (1967) La chromatographie en couche mince comme méthode de dédoublement des alcaloides racémiques. Application aux médicaments contenant de l’éphédrine. Ann. Pharm. Franc. 25, 177–180. 131. Wainer, I. , Brunner, C. , and Doyle, T. D. (1983) Direct resolution of enantiomers via thin-layer chromatography using a chiral adsorbent. J. Chromatogr. 264, 154. 132. Oi, N. (1985) Direct separation of optically active isomers by chromatographic methods. Farumashia, 21, 747–752.

1994) Adsorption chromatography on cellulose. XI. Chiral separations with aqueous solutions of cyclodextrins as eluents. J. Chromatogr. 659, 191–197. 86. Suedee, R. and Heard, C. M. (1997) Direct resolution of propranolol and bupranolol by thin-layer chromatography using cellulose derivatives as stationary phase. Chirality 9, 139–144. 87. , and Okamoto, Y. (2000) Tris(cyclohexylcarbamate)s of cellulose and amylose as potential chiral stationary phases for high-performance liquid chromatography and thin-layer chromatography.

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Chiral Separations: Methods and Protocols by Gerald Gübitz, Martin G. Schmid

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